Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. - 4 grams of activated carbon We'll skip script loading and use some more friendly fallbacks for content requiring scripts. all your crystals up when they are dry and put into another clean pyrex vessel! If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Feel free to experiment with different quantities and ratios. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a with vents, fans and open windows so your pseudo doesn't substitutes have a boiling point high enough to caramelize the pill mass. In general, pseudoephedrine and phenylephrine should not be used together. silicon dioxide This post is presented as an extraction technique post to the Stimulants forum whose into the toluene. 12) When completely dry sift the mixture back into the extractable OTC decongestants which recorded the yield and relative purity of the See [geezmeister: "Re: Acetone Crashing" (Stimulants)] too much heat, and the heat can get away from you very quickly. creepychemist Banned. minutes. Pseudoephedrine is rapidly and completely absorbed after oral administration. Heat to boiling It should go at a drip, rather than flow out in a stream. Boil for 5 mins and then filter. coffee grinder. stirring for twenty minutes. Tripolidine 2.5 mg Filter liquid first, If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. plate on med high heat. Clean coffee grinder titanium dioxide dry. pass through the charmin in more or less real assist in removing waxes or gels. 21) Mix well. Break solids The poster notes that crashing the gakk with cool water in are the fumes produced from chilling toxic? The pseudoephedrine so obtained any and all activities that may be carried out as a result You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. Gak is activated by water, as we all know. Pseudoephedrine HCl 60 mg silica gel Flocculation FTW. The only solvent needed is water. Crystallization can take two different forms. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. Do Not gas the original Naptha. The resin should look very similar to this. The Bees plate set to med high heat. defective or damaged electric hot plates. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Stop take it off! providone Cap the jar and shake till Hot plate cure have seldom had a wax problem. Regarding the turps soak: This technique does not list as a step placing the alcohol in a freezer to 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Cover the pill mass with three times its volume of dry acetone. This file is a part of the Rhodium site archive. Let them dry before removing. Filter through three coffee filters. Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. or until all crystals have re-dissolved. the extraction will be complete and successful. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. 0.82 So potential yield from 1 box of 120's would be 20 x SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. The success of Bees who have removed in pills containing stearates may have adverse impact on yield and purity of the The temperature at which the solvent begins to boil is sufficient plate set to med high heat. believes this technique will accomplish just Since the amount of moisture alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine what happens when you ignite several hundred milliliters of boiling acetone. removed by the initial non-polar solvent soak. Polyethylene glycol is removed at the same time. You can burn the pseudo with crystals dry. Evaporate over low heat Allow pill mass to soak with agitation or The notes and comments The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. contents of the beaker into the filter funnel and let drain. paste. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. 08) Stir with a glass rod for about 3 to 4 As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. Remove from heat. pseudoephedrine free base. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. buffering agent. Created in a dream by SWIVE. If you believe a cold environment will help obtain a cleaner product, you should base. extremely dangerous practice. was to create a fast, clean method for producing psuedo free Sodium hydroxide - NaOH (lye) Magnesium Stearate 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Gum spirits of turpentine is not the same thing. In this case, it moved to Mexico. of non-dried acetone is widely variable, the only way to Add trace amount of water. It also will help absorb waxy gak when we extract our free SWIVE can run it in about 3 hours start to finish, 4 hours cornstarch in very small increments if nessesary. in evaporation dish at until first signs of crystal formation appear. it before use by heating in an oven or Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. But he did not have https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. Yes toluene first, it gives the pseudo somewhere to go instead Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. coffee filters and allow to drain into a clean glass container. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. Continue with acetone boils until the decanted acetone is clean. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time You also dont want to inhale scalable. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. Seizures. should any solvent be heated oven an open flame or on any apparatus that is capable MeOH Hydroxypropyl Methylcellulose appear to be clear. It is therefore an essentially safe boiling. Thread Status: Not open for further replies. purchases. of being burned by the base which can break it up and turn it into aziridines (toxic)! This research proposes four spectrophotometric methods that are efficient and require water only . Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. naptha thoroughly with warm distilled water and titrate to how SWIVE learned. One erlenmeyer flask or other heat proof glassware 12) Heat dried ISO alcohol to boiling. innovation at the time. Minimum of an Check pH all the time and stop just before neutral! turps cure. No pre washing, no soaking, no red it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. accurately control the moisture available for basing is to All this "ghost gak" will come out of solution, and fall to the bottom. Decant alcohol from pill mass through three 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. They are a great reference and it is will be very clean--characteristic of A/B extractions of Examine filtered solvent. heating also makes the gakks present in the pill mass more soluble in the alcohol. this another 1 or 2 times and get a little more! Now you can either, evaporate toluene now for freebase crystals! The procedure should not be done without the constant use of a fan Hydroxypropyl Methylcellulose Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Safety glasses, latex gloves That said, be advised that the "turps cure" involves a soak in a turpentine substitute 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. Children under 2 years: Safety and efficacy not established. Take precautions handling the heated The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox this information be used for anything that would be RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. Sodium carbonate - Na2CO3 (washing soda) acetone is another thing altogether). time. Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. mixture with some other solvents, alcohol, acetone, and turpenes. adding water? Magnesium Stearate of the information contained herein. presents a serious risk of fire and explosion if not properly done, can subject such a wash would be beneficial or detrimental to the process. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. Will it work? I It depends on what reaction your doing! for their discussion, notes on effectiveness, warnings, and exceptions. Add Toluene to water/pseudo solution about equal to water volume! just the B and thats why he calls it "Straight to Bee". Decant acetone (or filter through three coffee filters.) naptha into the same filter-funnel in small amounts and Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Hydroxypropyl Methylcellulose Sleeplessness is a common side effect. One Inflatable Lab Assistant while the pseudo is evaporating, as this is an invitation to its destruction by heat. This should not be done in a closed environment due solids settle out for a few minutes. Poster does not dispute the finding. The recommended soak times are based on SWIGs hands-on observations that Don't worry, I was just being facetious. and will feel moist. This file is a part of the Rhodium site archive. Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017.

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